Dibenzyl azodicarboxylate synthesis
- Product Name:Dibenzyl azodicarboxylate
- CAS Number:2449-05-0
- Molecular formula:C16H14N2O4
- Molecular Weight:298.29
5394-50-3
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$172.00/50mg
2449-05-0
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$5.00/1g
Yield:2449-05-0 97%
Reaction Conditions:
with [bis(acetoxy)iodo]benzene in dichloromethane at 20; for 0.5 h;
Steps:
1 [Experimental Example 1]
PIDA (phenyliodine diacetate) and DCM (dichloromethane) were added to Compound 5, and the mixture was reacted with stirring at room temperature for 30 minutes to obtain DBAD (dibenzyl azodicarboxylate) in a yield of 97%.
References:
KR2021/153284,2021,A Location in patent:Paragraph 0269-0270; 0273-0274
501-53-1
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$10.00/1g
2449-05-0
252 suppliers
$5.00/1g