Dichloroacetyl chloride synthesis
- Product Name:Dichloroacetyl chloride
- CAS Number:79-36-7
- Molecular formula:C2HCl3O
- Molecular Weight:147.39
79-01-6
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$19.21/100ml
79-36-7
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$15.00/10g
Yield:79-36-7 90%
Reaction Conditions:
with tributyl borane;oxygen at 80; under 2280.15 Torr; for 11 h;Reagent/catalyst;
Steps:
1.1; 2.1; 3.1
Add 1314g (10mol) of trichloroethylene and 18.2g (0.1mol) of tributylboron into the pressure-resistant reactor, then pass in dry oxygen, adjust the pressure of the oxygen to 3 atmospheres, and then increase the temperature React at 80°C for 11h. After the completion of the reaction, atmospheric distillation is performed, and the fractions are collected at a temperature range of 105°C to 108°C to obtain 1,325 g of a colorless and transparent liquid product, dichloroacetyl chloride, with a yield of 90%.
References:
CN111995516,2020,A Location in patent:Paragraph 0041; 0043-0044; 0058; 0060-0061; 0066; 0068-0069
79-43-6
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79-36-7
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$15.00/10g
75-36-5
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$17.92/100G
79-36-7
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$15.00/10g
79-04-9
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$12.00/5g
76-02-8
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$38.29/25G
76-02-8
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79-36-7
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$15.00/10g
79-34-5
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$10.00/5g
79-36-7
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$15.00/10g
67-66-3
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$33.60/500ml
76-01-7
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