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ChemicalBook CAS DataBase List DICHLOROTRIS(2-METHOXYPHENYL)BISMUTH
121899-81-8

DICHLOROTRIS(2-METHOXYPHENYL)BISMUTH synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
1.2: 1 h / 10 - 30 °C
2.1: sulfuryl dichloride / chloroform / 0.5 h / 0 - 30 °C

References:

Nakashima, Yosuke;Jin, Yoshinobu;Konobe, Masato US2014/228219, 2014, A1

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