ChemicalBook CAS DataBase List Diethyl (trichloromethyl)phosphonate

Diethyl (trichloromethyl)phosphonate synthesis

14synthesis methods

Product Name:Diethyl (trichloromethyl)phosphonate
CAS Number:866-23-9
Molecular formula:C5H10Cl3O3P
Molecular Weight:255.46

Diethyl trichloromethylphosphonate was also obtained from diethyltrimethylsilyl phosphite in 60 % yield, and from benzyldiethyl phosphite in the presence of dibenzoyl peroxide and an ultraviolet source in a radical induced reaction in 87 % yield (compared to 26 % without the dibenzoyl peroxide).

56-23-5
0 suppliers
$18.50/48604

122-52-1
263 suppliers
$9.00/5g

866-23-9
77 suppliers
$15.00/1g

75-00-3
234 suppliers
$29.39/crm40015

Yield: 80 % Chromat. ， 90 % Chromat.

Reaction Conditions:

at 80; for 4 h;other activation: irradiation with UV light at 20 deg C;

References:

Bakkas, Salem;Julliard, Michel;Chanon, Michel [Tetrahedron,1987,vol. 43,# 3,p. 501 - 512]

56-23-5
0 suppliers
$18.50/48604

122-52-1
263 suppliers
$9.00/5g

866-23-9
77 suppliers
$15.00/1g

References

109-89-7
488 suppliers
$10.00/5g

122-52-1
263 suppliers
$9.00/5g

866-23-9
77 suppliers
$15.00/1g

78-40-0 Synthesis

78-40-0
567 suppliers
$5.00/25g

3167-69-9
0 suppliers
inquiry

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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inquiry

References

64-17-5 Synthesis

64-17-5
891 suppliers
$10.00/50g

21510-59-8
3 suppliers
inquiry

866-23-9
77 suppliers
$15.00/1g

References

56-23-5
0 suppliers
$18.50/48604

762-04-9
344 suppliers
$10.00/10 g

866-23-9
77 suppliers
$15.00/1g

References

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Diethyl (trichloromethyl)phosphonate synthesis

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