DIHYDROEUGENOL synthesis
- Product Name:DIHYDROEUGENOL
- CAS Number:2785-87-7
- Molecular formula:C10H14O2
- Molecular Weight:166.22
97-54-1
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2785-87-7
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$22.12/25G
Yield:2785-87-7 98%
Reaction Conditions:
with hydrogen in methanol at 20; for 20 h;chemoselective reaction;
Steps:
4.3. Typical procedure for the chemoselective hydrogenation
General procedure: The mixture of the substrate (0.250 mmol), 0.5% Pd/MS3A or 0.5% Pd/MS5A (10 wt % of the substrate) and MeOH (1 mL) was stirred under H2 atmosphere (balloon) at room temperature. After a given period, the reaction mixture was filtered through a membrane filter (Millipore, Millex-LH, 0.45 mm), and the filtrate was concentrated in vacuo to produce the corresponding reduced product.
References:
Takahashi, Tohru;Yoshimura, Masatoshi;Suzuka, Hiroyasu;Maegawa, Tomohiro;Sawama, Yoshinari;Monguchi, Yasunari;Sajiki, Hironao [Tetrahedron,2012,vol. 68,# 39,p. 8293 - 8299] Location in patent:experimental part
97-53-0
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2785-87-7
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92666-21-2
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2785-87-7
160 suppliers
$22.12/25G
97-53-0
804 suppliers
$5.00/25g
645-56-7
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$11.00/1g
2785-87-7
160 suppliers
$22.12/25G
52204-65-6
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$45.00/5g