Yield:923034-23-5 92%

Reaction Conditions:

with triethylamine;magnesium chloride in toluene; for 5 h;

References:

Payne, Joseph E.;Bonnefous, Celine;Hassig, Christian A.;Symons, Kent T.;Guo, Xin;Nguyen, Phan-Manh;Annable, Tami;Wash, Paul L.;Hoffman, Timothy Z.;Rao, Tadimeti S.;Shiau, Andrew K.;Malecha, James W.;Noble, Stewart A.;Hager, Jeffrey H.;Smith, Nicholas D. [Bioorganic and Medicinal Chemistry Letters,2008,vol. 18,# 23,p. 6093 - 6096] Location in patent:scheme or table Wash, Paul L.;Hoffman, Timothy Z.;Wiley, Brandon M.;Bonnefous, Celine;Smith, Nicholas D.;Sertic, Michael S.;Lawrence, Charles M.;Symons, Kent T.;Nguyen, Phan-Manh;Lustig, Kevin D.;Guo, Xin;Annable, Tami;Noble, Stewart A.;Hager, Jeffrey H.;Hassig, Christian A.;Malecha, James W. [Bioorganic and Medicinal Chemistry Letters,2008,vol. 18,# 24,p. 6482 - 6485] Location in patent:scheme or table