Dimethylglyoxime synthesis
- Product Name:Dimethylglyoxime
- CAS Number:95-45-4
- Molecular formula:C4H8N2O2
- Molecular Weight:116.12
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Yield:-
Reaction Conditions:
with ammonium hydroxide;dihydrogen peroxide in ethanol at 40; for 1 h;Temperature;
Steps:
2 Example 2
A constant temperature reaction temperature of 30 ° C was set, 2.0 g of TS-1, 0.5 g of butanedione and 5.0 g of ethanol were added to a three-Constant pressure dropping funnel 1.1 g of concentrated aqueous ammonia solution (25%) and 1.3 g of hydrogen peroxide (30%) were added in three portions over 0.5 h. Start drippingPlus time, reaction 0.5h. The Ti-Si molecular sieve TS-1 was selected to be 0.8 g, the same as in Example 1
References:
CN106543031,2017,A Location in patent:Paragraph 0033; 0034-0042; 0045-0052; 0055-00081
431-03-8
387 suppliers
$17.00/25mL
95-45-4
523 suppliers
$15.00/25g
431-03-8
387 suppliers
$17.00/25mL
64-19-7
1679 suppliers
$10.00/25ML
95-45-4
523 suppliers
$15.00/25g
135636-66-7
0 suppliers
inquiry
95-45-4
523 suppliers
$15.00/25g
