Diphenylsilanediol synthesis
- Product Name:Diphenylsilanediol
- CAS Number:947-42-2
- Molecular formula:C12H12O2Si
- Molecular Weight:216.31
775-12-2
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947-42-2
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Yield:947-42-2 99%
Reaction Conditions:
with oxygen in water;acetone at 30; under 760.051 Torr; for 0.333333 h;
Steps:
4) Typical reaction procedure
General procedure: A typical reaction procedure for the oxidation of 1 to 2 using Au/HAP was as follows.Au/HAP (0.005 g, Au: 0.0415 mol%) was placed in a reaction vessel (50 cm3), followedby the addition of acetone (4 mL), water (0.1 mL), and 1 (1 mmol). The reactionmixture was vigorously stirred at 30 °C under O2 atmosphere for 7 min. Au/HAP wasfiltered and the yield was determined by GC analysis. The product was isolated byKugelrohr distillation.
References:
Urayama, Teppei;Mitsudome, Takato;Maeno, Zen;Mizugaki, Tomoo;Jitsukawa, Koichiro;Kaneda, Kiyotomi [Chemistry Letters,2015,vol. 44,# 8,p. 1062 - 1064] Location in patent:supporting information
5906-79-6
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80-10-4
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18676-80-7
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947-42-2
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775-12-2
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$10.00/1g
947-42-2
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1333-74-0
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