DIVINYL SEBACATE synthesis
- Product Name:DIVINYL SEBACATE
- CAS Number:10355-50-7
- Molecular formula:C14H22O4
- Molecular Weight:254.32
Yield:10355-50-7 100%
Reaction Conditions:
with sulfuric acid;mercury(II) diacetate at 20 - 50; for 4 h;
Steps:
Synthesis of Divinyl Esters.
Divinyl esters of adipic,sebacic, dodecanedioic, tridecanedioic acid were synthesizedby the transvinylation reaction of acid with an excess ofvinyl propionate by using mercuric acetate and sulfuric acidas catalysts.22 In all cases product was purified by columnchromatography with hexane containing 2 % ethyl acetate.Product yield was more than 90 % in all cases.
References:
Ashrafuzzaman, Md.;Pyo, Jung In;Cheong, Chan Seong [Bulletin of the Korean Chemical Society,2014,vol. 35,# 2,p. 477 - 482] Location in patent:supporting information
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