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Doqualast synthesis

1synthesis methods

201230-82-2 Synthesis

Yield:64019-03-0 48%

Reaction Conditions:

with calcium hydroxide;nickel carbonyl;water in N,N-dimethyl-formamide at 110 - 115; under 2068.6 Torr;

References:

Tilley;LeMahieu;Carson;Kierstead;Baruth;Yaremko [Journal of Medicinal Chemistry,1980,vol. 23,# 1,p. 92 - 95]

2-AMINO-5-METHYLBENZAMIDE

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