Ethanone, 1-(2-chloro-5-hydroxyphenyl)- synthesis
- Product Name:Ethanone, 1-(2-chloro-5-hydroxyphenyl)-
- CAS Number:58020-38-5
- Molecular formula:C8H7ClO2
- Molecular Weight:170.59
121-71-1
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$5.00/5g
58020-38-5
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$65.00/5mg
69240-96-6
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61124-56-9
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Yield:58020-38-5 33%
Reaction Conditions:
Stage #1: 3-Hydroxyacetophenonewith toluene-4-sulfonic acid in water;acetonitrile at 20; for 0.0833333 h;
Stage #2: with N-chloro-succinimide in water;acetonitrile at 20; for 2 h;regioselective reaction;
References:
Bovonsombat, Pakorn;Ali, Rameez;Khan, Chiraphorn;Leykajarakul, Juthamard;Pla-On, Kawin;Aphimanchindakul, Suraj;Pungcharoenpong, Natchapon;Timsuea, Nisit;Arunrat, Anchalee;Punpongjareorn, Napat [Tetrahedron,2010,vol. 66,# 34,p. 6928 - 6935] Location in patent:experimental part
77344-69-5
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$200.00/100mg
58020-38-5
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$65.00/5mg
6280-89-3
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$7.00/250mg
58020-38-5
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$65.00/5mg