H-DL-ASP(OME)-OH HCL synthesis
- Product Name:H-DL-ASP(OME)-OH HCL
- CAS Number:1835-52-5
- Molecular formula:C5H10ClNO4
- Molecular Weight:183.59
67-56-1
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$7.29/5ml-f
617-45-8
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$5.00/25g
1835-52-5
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$11.00/250mg
Yield: 98%
Reaction Conditions:
Stage #1:methanol with acetyl chloride at 0; for 1 h;
Stage #2:aspartic Acid with hydrogenchloride at 0 - 20;
References:
Mandai, Hiroki;Hongo, Kohei;Fujiwara, Takuma;Fujii, Kazuki;Mitsudo, Koichi;Suga, Seiji [Organic Letters,2018,vol. 20,# 16,p. 4811 - 4814] Location in patent:supporting information