H-GLU(ANILIDE)-OH synthesis
- Product Name:H-GLU(ANILIDE)-OH
- CAS Number:5963-60-0
- Molecular formula:C11H14N2O3
- Molecular Weight:222.24
56-86-0
919 suppliers
$5.00/25g
5963-60-0
33 suppliers
$45.00/25mg
Yield:-
Steps:
Multi-step reaction with 6 steps
1: 98 percent / triethylamine / methanol / 3 h
2: 90 percent / toluenesulfonic acid / toluene / 3 h / Heating
3: thionyl chloride / CH2Cl2 / 0.5 h / Heating
4: pyridine / CH2Cl2 / 0.25 h / 20 °C
5: lithium hydroxide / tetrahydrofuran; H2O / 0.5 h / 5 °C
6: hydrogen / Pd/C / methanol
References:
Esslinger, C. Sean;Cybulski, Kimberly A.;Rhoderick, Joseph F. [Bioorganic and Medicinal Chemistry,2005,vol. 13,# 4,p. 1111 - 1118]
![L-Glutamine, N-phenyl-N2-[(phenylmethoxy)carbonyl]-](/CAS/20210111/GIF/110336-85-1.gif)
110336-85-1
0 suppliers
inquiry
5963-60-0
33 suppliers
$45.00/25mg
![3-Oxazolidinecarboxylic acid, 5-oxo-4-[3-oxo-3-(phenylamino)propyl]-, phenylmethyl ester, (4S)-](/CAS/20210305/GIF/848215-07-6.gif)
848215-07-6
0 suppliers
inquiry
5963-60-0
33 suppliers
$45.00/25mg
1155-62-0
364 suppliers
$10.00/5g
5963-60-0
33 suppliers
$45.00/25mg
58456-26-1
2 suppliers
inquiry
5963-60-0
33 suppliers
$45.00/25mg