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ChemicalBook CAS DataBase List Hexachloro-1,3-butadiene
87-68-3

Hexachloro-1,3-butadiene synthesis

14synthesis methods
-

Yield:-

Reaction Conditions:

with zinc(II) chloride at 100; for 12 h;Autoclave;

Steps:

2 Comparative Example 2

Separately using tetrachlorethylene as raw material,81.5 g of tetrachlorethylene was weighed in a hydrothermal autoclave, 12.2 g of anhydrous zinc chloride was added at a mass fraction of 15%, reacted at a reaction temperature of 100 ° C for 12 h,The conversion of tetrachlorethylene was 24% and the selectivity of hexachloro-1,3-butadiene was 21%.

References:

CN106966859,2017,A Location in patent:Paragraph 0015; 0022

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