ChemicalBook CAS DataBase List HYDROXYHEXAMIDE

HYDROXYHEXAMIDE synthesis

6synthesis methods

Product Name:HYDROXYHEXAMIDE
CAS Number:3168-01-2
Molecular formula:C15H22N2O4S
Molecular Weight:326.41

1565-17-9
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3168-01-2
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 95 percent / NaBH₄ / methanol / 0.5 h / 0 °C
2: 87 percent / pyridine / 2 h / -10 °C
3: 1.) 1,8-diazabicyclo<5.4.0>undec-7-ene / 1.) benzene, RT, 30 min, 2.) benzene, RT, 1 h
4: 90 percent / K₂CO₃, MeOH / 12 h / Ambient temperature

References:

Akita, Hiroyuki;Kurashima, Katsumi;Nozawa, Masako;Yamamura, Shigeo;Seri, Kenzi;Imamura, Yorishige [Tetrahedron Asymmetry,1998,vol. 9,# 24,p. 4331 - 4340]

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968-81-0
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3168-01-2
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References

16712-69-9 Synthesis

16712-69-9
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$12.00/1g

3168-01-2
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References

138-38-5
123 suppliers
$11.00/5g

3168-01-2
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References

113412-15-0 Synthesis

113412-15-0
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3168-01-2
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References

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HYDROXYHEXAMIDE synthesis