ChemicalBook CAS DataBase List hypoglycin

hypoglycin synthesis

4synthesis methods

Product Name:hypoglycin
CAS Number:156-56-9
Molecular formula:C7H11NO2
Molecular Weight:141.17

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156-56-9
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 65 percent / pyridine, p-toluenesulfonyl chloride / CCl₄; diethyl ether / 21 h / Ambient temperature; 1.) 0 deg C
2: 90 percent / n-BuLi / tetrahydrofuran; hexane / -78 deg C, 2 h 25 min, then room temp., 2 h 25 min
3: 0.25M HCl / H₂O / 70 h / Ambient temperature
4: LiOH*H₂O / tetrahydrofuran; H₂O / 24 h / Ambient temperature

References:

Baldwin, Jack E.;Adlington, Robert M.;Bebbington, David;Russell, Andrew T. [Tetrahedron,1994,vol. 50,# 41,p. 12015 - 12028]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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156-56-9
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References

1000210-73-0
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156-56-9
22 suppliers
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References

1000210-73-0
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156-56-9
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References

hypoglycin Related Search:

2-Cyclopropyl ethylamine (free base) METHYLENECYCLOPROPANE; >98%DISCONTINUED

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hypoglycin synthesis

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