isocyanatocyclobutane synthesis
- Product Name:isocyanatocyclobutane
- CAS Number:5811-25-6
- Molecular formula:C5H7NO
- Molecular Weight:97.12
Yield:-
Reaction Conditions:
with N-ethyl-N,N-diisopropylamine in tetrahydrofuran at 0; for 0.5 h;
Steps:
71.B
A solution of cyclobutylamine (71 mg, 1.0 mmol) and DIPEA (3.0 mmol) in 5 mL THF was slowly added to a solution of triphosgene (105 mg, 0.35 mmol) in 10 mL EPO
References:
WO2006/33633,2006,A1 Location in patent:Page/Page column 101; 102
1033694-56-2
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