ChemicalBook CAS DataBase List Isoeleutherin

Isoeleutherin synthesis

4synthesis methods

Product Name:Isoeleutherin
CAS Number:1078723-14-4
Molecular formula:C16H16O4
Molecular Weight:272.3

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.42 h / 0 - 20 °C / Inert atmosphere
1.2: 2 h / 0 - 20 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
2.2: 0.5 h
3.1: boron trifluoride diethyl etherate / dichloromethane / 10 h / 20 °C / Inert atmosphere
4.1: ammonium cerium (IV) nitrate / water; acetonitrile / 1 h / 20 °C

References:

Fernandes, Rodney A.;Chavan, Vijay P.;Mulay, Sandip V. [Tetrahedron Asymmetry,2011,vol. 22,# 4,p. 487 - 492]

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1078723-14-4
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References

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1078723-14-4
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References

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1078723-14-4
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References

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Isoeleutherin synthesis

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