ISOPROPYL CYCLOPROPANE CARBOXYLATE synthesis
- Product Name:ISOPROPYL CYCLOPROPANE CARBOXYLATE
- CAS Number:6887-83-8
- Molecular formula:C7H12O2
- Molecular Weight:128.17
3153-34-2
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6887-83-8
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Yield:6887-83-8 80%
Reaction Conditions:
with methyl tributylammonium chloride;sodium hydroxide at 25; for 6 h;
Steps:
12
To the three port in the round-bottom flask, input Sodium hydroxide and methyltri-butyl ammonium chloride, the molar ratio of the inputs: 1: 1.5 : 0.063, wherein X is Cl, R is isopropyl. Keep the reactant temperature is 25 °C, uniform stirring, reaction 6 hours, after filtering, the filtrate, rectifying and separating the finished product. In the finished product using gas chromatography to measure the weight of product content is 85%, the weight is calculated according to the yield of 80%.
References:
CN105906507,2016,A Location in patent:Paragraph 0045; 0046
