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ChemicalBook CAS DataBase List L-Alanyl-L-alanine
1948-31-8

L-Alanyl-L-alanine synthesis

7synthesis methods
-

Yield:-

Reaction Conditions:

with Sodium trimetaphosphate in aq. buffer; pH=10.7 at 37; under 225023 Torr;Pressure;Temperature;

Steps:

General conditions for the reaction of amino acids with P3m
General procedure: Typical conditions for the reactions: 0.1 M amino acid (Phe, Trp, Met, Val, Gly and Ala) and 0.1 M Trimetaphosphate (P3m). The reactions were carried out under 1 bar and 300 bar at two temperatures, 26 °C and 37 °C, in aqueous solution with the pH 10.7 for 7 days, respectively. The reactions were quenched by adjusting the pH to 4~5 using HCl. The resulting reaction mixtures were then analyzed by HPLC-MS.

References:

Ying, Jianxi;Chen, Peng;Wu, Yile;Yang, Xu;Yan, Kaili;Xu, Pengxiang;Zhao, Yufen [Chinese Chemical Letters,2019,p. 367 - 370] Location in patent:supporting information

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