LUMICHROME synthesis
- Product Name:LUMICHROME
- CAS Number:1086-80-2
- Molecular formula:C12H10N4O2
- Molecular Weight:242.23
61127-23-9
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3171-45-7
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1086-80-2
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Yield:1086-80-2 55%
Reaction Conditions:
with toluene-4-sulfonic acid for 1 h;Milling;
Steps:
7,8-Dimethylalloxazine (36) [22]
Mixture of alloxan monohydrate (100 mg, 0.62 mmol), 4,5-dimethyl-1,2-phenylenediamine (85mg, 0.62 mmol) and p-toluenesulfonic acid (119 mg, 0.62 mmol) was placed in a stainless steelgrinding jar (10 mL) with one 12 mm stainless steel ball and milled for one hour at 30 Hz. Uponcompletion, the reaction mixture was washed with methanol and filtered. The product wasobtained as yellow solid (83 mg, 55%).
References:
Bri?, Anamarija;Dud, Mateja;Margeti?, Davor [Beilstein Journal of Organic Chemistry,2017,vol. 13,p. 1745 - 1752] Location in patent:supporting information
83-88-5
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1086-80-2
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1088-56-8
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83-88-5
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1086-80-2
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![Carbamic acid, [3-(aminocarbonyl)-6,7-dimethyl-2-quinoxalinyl]-, ethyl ester (9CI)](/CAS/20200119/GIF/80144-39-4.gif)
80144-39-4
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1086-80-2
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4250-90-2
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1086-80-2
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