Methyl 3-aminocrotonate synthesis
- Product Name:Methyl 3-aminocrotonate
- CAS Number:14205-39-1
- Molecular formula:C5H9NO2
- Molecular Weight:115.13
105-45-3
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$5.00/5g
14205-39-1
508 suppliers
$6.00/25g
Yield:14205-39-1 94%
Reaction Conditions:
with ammonia;acetic acidProduct distribution / selectivity;
Steps:
5
Example 5: Process for the preparation of methyl amino crotonate Continuous flow experiment was carried out in a SS316 tubular reactor of 6.35 mm o.d. and 2 m length at 50 e C with a residence time of 120 - 160 s without any solvent. The Methyl aceto acetate to ammonia to catalyst (Acetic acid)- volume ratio of 1:3:0.5 yielded 94% methyl amino crotonate from the first crop. No choking of reactor was observed.
References:
COUNCIL OF SCIENTIFIC & INDUSTRIAL RESEARCH;KULKARNI, Amol, Arvind;JOSHI, Ramesh, Anna;JOSHI, Rohini, Ramesh WO2012/147103, 2012, A2 Location in patent:Page/Page column 6-7
7664-41-7
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105-45-3
703 suppliers
$5.00/5g
14205-39-1
508 suppliers
$6.00/25g
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14205-39-1
508 suppliers
$6.00/25g
105-45-3
703 suppliers
$5.00/5g
5977-14-0
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$35.70/100g
14205-39-1
508 suppliers
$6.00/25g