METHYL-D3-ACETYLENE synthesis
- Product Name:METHYL-D3-ACETYLENE
- CAS Number:13025-73-5
- Molecular formula:C3H4
- Molecular Weight:40.07
Yield:-
Reaction Conditions:
Stage #1: acetylenewith n-butyllithium in tetrahydrofuran at -78; for 0.5 h;Metallation;
Stage #2: d6-dimethyl sulfate in tetrahydrofuran at -40 - -10; for 2.5 h;Further stages.;Methylation;
References:
Boullais, Claude;Rannou, Christelle;Reveillere, Emmanuel;Mioskowski, Charles [European Journal of Organic Chemistry,2000,# 5,p. 723 - 727]
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