METHYL PERFLUOROOCTANOATE synthesis
- Product Name:METHYL PERFLUOROOCTANOATE
- CAS Number:376-27-2
- Molecular formula:C9H3F15O2
- Molecular Weight:428.1
67-56-1
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$7.29/5ml-f
335-67-1
334 suppliers
$10.00/1 g
376-27-2
104 suppliers
$10.00/2 g
Yield:376-27-2 89%
Reaction Conditions:
with sulfuric acid for 4 h;Heating / reflux;
Steps:
2.i
EXAMPLE 2; Synthesis of perfluoro-N1 , N7 -dioctanimidoylheptanediimidamide (DPIA-56); (i) Methyl perfluorooctanoate; A 2-1, four-necked, round-bottomed flask equipped with stirrer, addition funnel, thermometer and reflux condenser, is charged with 828 g (2 mol) of dried perfluorooctanoic acid, 16O g (5 mol) of methanol. The mixture is stirred and 50 ml concentrated sulfuric acid is added dropwise. Then the mixture is heated to reflux for 4 hr. At the end of the reflux period the
References:
LODESTAR INC. WO2008/8316, 2008, A2 Location in patent:Page/Page column 29-30
111-11-5
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376-27-2
104 suppliers
$10.00/2 g
67-56-1
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$7.29/5ml-f
3825-26-1
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$45.00/5 g
376-27-2
104 suppliers
$10.00/2 g
67-56-1
803 suppliers
$7.29/5ml-f
335-64-8
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$15.00/2 g
376-27-2
104 suppliers
$10.00/2 g
307-35-7
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$35.00/10 g
376-27-2
104 suppliers
$10.00/2 g