ChemicalBook CAS DataBase List MONOCROTALINE

MONOCROTALINE synthesis

7synthesis methods

Product Name:MONOCROTALINE
CAS Number:315-22-0
Molecular formula:C16H23NO6
Molecular Weight:325.36

1,3-Dioxolane-4-acetic acid, α,4,5-trimethyl-5-[[2-(trimethylsilyl)ethoxy]carbonyl]-, 2,3,5,7a-tetrahydro-7-(hydroxymethyl)-1H-pyrrolizin-1-yl ester, [1α[R*(4R*,5R*)],7aβ]- (9CI)

109391-29-9
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315-22-0
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: Et₃N / CH₂Cl₂
2: 71 percent / Bu₄N⁽¹⁺⁾F^(1-)*3H₂O / acetonitrile / 34 °C
3: 75 percent / 38percent HCl / ethane-1,2-diol / 2 h / 110 °C

References:

Vedejs;Ahmad;Larsen;Westwood [Journal of Organic Chemistry,1987,vol. 52,# 17,p. 3937 - 3938]

(13R,14R)-14,19-Dihydro-12,13-dihydroxy-20-norcrotalanan-11,15-dione 4-oxide

35337-98-5
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315-22-0
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$35.00/10mg

References

1,3-Dioxolane-4-acetic acid, α,4,5-trimethyl-5-[[2-(trimethylsilyl)ethoxy]carbonyl]-, 7-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2,3,5,7a-tetrahydro-1H-pyrrolizin-1-yl ester, [4α[αR*(1R*,7aR*)],5α]- (9CI)

109432-25-9
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315-22-0
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$35.00/10mg

References

1H-Pyrrolizin-1-ol, 7-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2,3,5,7a-tetrahydro-, lithium salt (1:1), (1R,7aR)-rel-

89710-47-4
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315-22-0
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$35.00/10mg

References

D-erythro-Pent-4-enitol, 4,5-dideoxy-4-methyl-2,3-di-C-methyl-2,3-O-methylene-, α-methoxy-α-(trifluoromethyl)benzeneacetate, (R)- (9CI)

121719-94-6
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315-22-0
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References

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MONOCROTALINE synthesis

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