N-(4-METHOXYBENZYLIDENE)ANILINE synthesis
- Product Name:N-(4-METHOXYBENZYLIDENE)ANILINE
- CAS Number:836-41-9
- Molecular formula:C14H13NO
- Molecular Weight:211.26
Yield: 92%
Reaction Conditions:
with C26H21BiClN in chloroform at 100; for 10 h;Reagent/catalyst;
Steps:
35 Catalytic activity test:
Add 0.5 mmol of phenylacetylene to the 10 mL reaction tube (R1, R2, R4, R5 are hydrogen, R3 is methoxy), 0.5 mmol aniline(R6, R7, R8, R9, R10 are hydrogen),0.015 mmol of the novel organic rhodium complex catalyst obtained in Example 35,Then add 2ml of chloroform,The reaction tube was placed in a heater at 100 ° C for 10 h.After the reaction is completed,The target compound is isolated by column chromatography.The yield was 92%.
References:
Hunan University;Qiu Renhua;Zhang Dejiang CN109206453, 2019, A Location in patent:Paragraph 0169; 0170; 0172; 0173; 0177; 0181
3526-43-0
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3526-43-0
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$41.00/250mg
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$29.00/5g