NSC47034 synthesis
- Product Name:NSC47034
- CAS Number:6952-67-6
- Molecular formula:C9H9NO4
- Molecular Weight:195.17
Yield:6952-67-6 100%
Reaction Conditions:
with toluene-4-sulfonic acid in ethylene glycol;benzene;
Steps:
3.3 (3-3)
A mixture of 3-nitrobenzaldehyde (100 g, 0.66 mole), ethylene glycol (49.3 g, 0.7 mole) and p-toluenesulfonic acid (0.8 g) and benzene (1 L) was heated at reflux with continuous removal of water via a Dean and Stark trap. After 4 hours, the mixture was cooled, filtered through a pad of neutral alumina and concentrated in vacuo to afford 2-(3-nitrophenyl)-1,3-dioxolane (130.4 g, 100%) as an amber oil used without further purification below. Step (b) 2-(3-Aminophenyl)-1,3-dioxolane
References:
US4701459,1987,A
99-61-6
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![Ethanol, 2-[(3-nitrophenyl)methoxy]-](/CAS/20210305/GIF/96206-46-1.gif)
96206-46-1
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