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ChemicalBook CAS DataBase List OTAVA-BB 1361129
81471-20-7

OTAVA-BB 1361129 synthesis

12synthesis methods
1H-Indole, 2,3-dibromo-1-methyl-

128746-62-3
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Yield:81471-20-7 99%

Reaction Conditions:

Stage #1: 2,3-dibromo-1-methyl-1H-indolewith tert.-butyl lithium in tetrahydrofuran;hexane at -78; for 0.0833333 h;
Stage #2: with water;ammonium chloride in tetrahydrofuran;hexane at -78 - 20;

References:

Liu, Yanbing;Gribble, Gordon W [Tetrahedron Letters,2002,vol. 43,# 40,p. 7135 - 7137]

OTAVA-BB 1361129 Related Search:

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