P-DECYLOXYNITROBENZENE synthesis
- Product Name:P-DECYLOXYNITROBENZENE
- CAS Number:31657-37-1
- Molecular formula:C16H25NO3
- Molecular Weight:279.37
112-30-1
520 suppliers
$5.00/25g
100-00-5
73 suppliers
$14.00/25g
31657-37-1
17 suppliers
$106.00/250mg
Yield:31657-37-1 95 %
Reaction Conditions:
with caesium carbonate in toluene at 80;
Steps:
General procedure for C-O cross-coupling reaction:
General procedure: In a reaction tube Pd catalyst (25 mg), Cs2CO3 (1.2 mmol, 0.165 g), Toluene (2 mL), arylhalide (1 mmol) and alcohol (1.2 mmol) were added and this mixture was heated whilst keep on stirring at 80 °C. After 6h the reaction mixture was stopped and the reaction mixture was cooled at room temperature. The organic layer was extracted in the solution mixture of water and ethylacetate, organic layer was dried under reduced pressure and the resulting residue was subjected for the column chromatographic separation of the final product which was further confirmed by the 1H NMR and 13C NMR spectroscopy.
References:
Khandaka, Himanshu;Kumar Joshi, Raj [Tetrahedron Letters,2022,vol. 111,art. no. 154163] Location in patent:supporting information
100-02-7
95 suppliers
$11.00/5G
112-29-8
420 suppliers
$6.00/25g
31657-37-1
17 suppliers
$106.00/250mg
100-02-7
95 suppliers
$11.00/5G
2050-77-3
155 suppliers
$19.00/5g
31657-37-1
17 suppliers
$106.00/250mg
249648-28-0
0 suppliers
inquiry
31657-37-1
17 suppliers
$106.00/250mg
112-29-8
420 suppliers
$6.00/25g
98-95-3
39 suppliers
$14.00/25g
31657-37-1
17 suppliers
$106.00/250mg