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ChemicalBook CAS DataBase List (Pentafluorophenyl)dimethylphosphine
5075-61-6

(Pentafluorophenyl)dimethylphosphine synthesis

3synthesis methods
-

Yield:5075-61-6 85%

Reaction Conditions:

Stage #1: Pentafluorobenzenewith n-butyllithium in diethyl ether;hexane at -78; for 1 h;
Stage #2: dimethyl chlorophosphine in diethyl ether at -78 - 20; for 12 h;

References:

Müller, Felix;Mix, Andreas;Stammler, Hans-Georg;Mitzel, Norbert W. [European Journal of Inorganic Chemistry,2022,vol. 2022,# 11,art. no. E202101083]

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