Phenyl vinyl sulfone synthesis
- Product Name:Phenyl vinyl sulfone
- CAS Number:5535-48-8
- Molecular formula:C8H8O2S
- Molecular Weight:168.21
1822-73-7
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$24.00/1g
5535-48-8
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$12.00/1g
Yield:5535-48-8 99%
Reaction Conditions:
with C4H9N2O9W in methanol;water at 20; for 4 h;chemoselective reaction;
Steps:
General procedure for oxidation of sulfides to sulfones: To a stirred solution of sulfide (1.25 mmol) in CH3OH/H2O (1:1, 10 mL), the complex MWG (1.17 g, 2.5 mmol) or DWC (1.12 g, 1.25 mmol) or DWG (1.13 g, 1.25 mmol) were added successively maintaining molar ratio of W:substrate at 2:1. After completion of the reaction, the sulfone obtained was isolated, purified, and characterized by methods similar to those described under the procedure for oxidation of sulfide to sulfoxide.
References:
Das, Siva Prasad;Boruah, Jeena Jyoti;Chetry, Hiran;Islam, Nashreen S. [Tetrahedron Letters,2012,vol. 53,# 9,p. 1163 - 1168] Location in patent:experimental part
20451-53-0
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$60.00/100mg
5535-48-8
271 suppliers
$12.00/1g
1822-73-7
106 suppliers
$24.00/1g
5535-48-8
271 suppliers
$12.00/1g
20451-53-0
85 suppliers
$60.00/100mg
20611-21-6
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$29.00/1g
5535-48-8
271 suppliers
$12.00/1g
31469-08-6
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100-58-3
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$18.00/10ml
5535-48-8
271 suppliers
$12.00/1g