PHENYLETHYNYLDIMETHYLSILANE synthesis
- Product Name:PHENYLETHYNYLDIMETHYLSILANE
- CAS Number:87290-97-9
- Molecular formula:C10H12Si
- Molecular Weight:160.29
1066-35-9
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Yield:87290-97-9 98%
Reaction Conditions:
Stage #1: phenylacetylenewith ethylmagnesium bromide in tetrahydrofuran;diethyl ether at 0 - 20; for 0.0833333 h;Inert atmosphere;
Stage #2: Chlorodimethylsilan in tetrahydrofuran;diethyl ether at 0 - 20; for 4 h;Inert atmosphere;
References:
Muchnij, Jill A.;Kwaramba, Farai B.;Rahaim, Ronald J. [Organic Letters,2014,vol. 16,# 5,p. 1330 - 1333] Location in patent:supporting information
6738-06-3
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1066-35-9
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113403-33-1
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536-74-3
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1825-61-2
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18107-29-4
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1066-35-9
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4440-01-1
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