PIPERIDINE-3-BORONIC ACID synthesis
1synthesis methods
- Product Name:PIPERIDINE-3-BORONIC ACID
- CAS Number:120347-74-2
- Molecular formula:C5H12BNO2
- Molecular Weight:128.97
Yield:-
Reaction Conditions:
with dimethylsulfide borane complex in tetrahydrofuran;mixing of compd. (0°C, Ar atmosphere), stirring of mixt. (1h, room temp.), evapn., addn. of cold CH3OH, stirring under reflux (30 min), evapn., dissolving (HCl), refluxing (1h), evapn. (vac., 60°C, percolating ion exchange resin; evapn.;
References:
Dicko, Amadou;Montury, Michel;Baboulene, Michel [Synthetic Communications,1988,vol. 18,# 5,p. 459 - 464]