piro[2.5]octan-6-ol synthesis
- Product Name:piro[2.5]octan-6-ol
- CAS Number:22428-83-7
- Molecular formula:C8H14O
- Molecular Weight:126.2
13482-22-9
208 suppliers
$8.00/250mg
22428-83-7
47 suppliers
$695.00/250mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 50 °C / Inert atmosphere
2.1: sodium t-butanolate / tetrahydrofuran / 1 h / 20 °C
2.2: 18 h / 20 °C
3.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere
References:
BIOMARIN PHARMACEUTICAL INC.;WANG, Bing;CHAO, Qi WO2019/133770, 2019, A2
![CYCLOHEXANONE, 4-[[(1,1-DIMETHYLETHYL)DIPHENYLSILYL]OXY]-](/CAS/GIF/130745-59-4.gif)
130745-59-4
23 suppliers
$133.00/500mg
22428-83-7
47 suppliers
$695.00/250mg