PYRIDINE-2-D1 synthesis
- Product Name:PYRIDINE-2-D1
- CAS Number:1807-97-2
- Molecular formula:C5H5N
- Molecular Weight:79.1
109-09-1
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$10.60/1gm:
1807-97-2
13 suppliers
$490.00/500mg
Yield:1807-97-2 > 98 %Chromat.
Reaction Conditions:
with triethanolamine;ethyl [2]alcohol;water-d2 for 24 h;Irradiation;Glovebox;
Steps:
2.7 General procedure of photocatalytic reactions
General procedure: A silica tube containing the catalyst, substrate (0.2 mmol), TEOA (0.9 mL), H2O (8.1 mL) and ethanol (1 mL), was sealed in a glovebox and transferred outside. Then the mixture was irradiated under the LED light (427 nm) with stirring for 24 h. Ether acetate (5 mL) was added to the mixture and the upper organic phase was collected. The yield was calculated by GC-MS with the standard curve and by NMR. For photocatalytic stability evaluation, the catalyst was re-collected by centrifugation, washed with ethanol and dried under vacuum. For deuteration, D2O and CH2CH2OD were used instead of water and ethanol.
References:
Ling, Xiang;Xu, Yangsen;Wu, Shaoping;Liu, Mofan;Yang, Peng;Qiu, Chuntian;Zhang, Guoqiang;Zhou, Hongwei;Su, Chenliang [Science China Chemistry,2020,vol. 63,# 3,p. 386 - 392]
109-04-6
527 suppliers
$6.00/25g
1807-97-2
13 suppliers
$490.00/500mg
![Pyridinium, 1-[2,2,2-trifluoro-1-hydroxy-1-(trifluoromethyl)ethyl]-, inner salt](/CAS/20211123/GIF/87432-74-4.gif)
87432-74-4
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1807-97-2
13 suppliers
$490.00/500mg
110-86-1
889 suppliers
$9.00/5g
1455-13-6
127 suppliers
$34.00/25ml
1807-97-2
13 suppliers
$490.00/500mg
110-86-1
889 suppliers
$9.00/5g
1807-97-2
13 suppliers
$490.00/500mg