(R)-4-BROMOSTYRENE OXIDE synthesis
- Product Name:(R)-4-BROMOSTYRENE OXIDE
- CAS Number:62566-68-1
- Molecular formula:C8H7BrO
- Molecular Weight:199.04
96855-38-8
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62566-68-1
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Yield: 98%
Reaction Conditions:
with sodium hydroxide in tetrahydrofuran;water at 20; for 1 h;enantioselective reaction;
Steps:
General procedure for the synthesis of chiral styrene oxides
General procedure: For the preparation of chiral styrene oxides, 3 mL NaOH(2 N) was added to α-bromohydrin (0.5 mmol) in 6 mL tetrahydrofuran(THF) and then was sttired at room temperature for 1 h. After completing the reaction, the product was extracted by EtOAc and then purified using column chromatography on silica gel using ethyl acetate/n-hexane gradient to give the desired product in high purity.
References:
Hosseinzadeh, Rahman;Mohadjerani, Maryam;Mesgar, Sakineh [Journal of the Iranian Chemical Society,2019,vol. 16,# 3,p. 583 - 591]
1029431-48-8
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62566-68-1
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32017-76-8
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62566-68-1
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100306-24-9
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99-73-0
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$10.00/1g
62566-68-1
45 suppliers
$65.00/50mg