ChemicalBook CAS DataBase List (S)-1-Boc-3-hydroxymethyl-piperazine

(S)-1-Boc-3-hydroxymethyl-piperazine synthesis

9synthesis methods

Product Name:(S)-1-Boc-3-hydroxymethyl-piperazine
CAS Number:314741-40-7
Molecular formula:C10H20N2O3
Molecular Weight:216.28

(S) -1-BOC-3-hydroxymethylpiperazine can be used as an intermediate in organic synthesis, which can be synthesized from (S)-(4-benzylpiperazine-2-yl) methanol and methanol,with Palladium hydroxide on carbon.

147650-70-2 Synthesis

147650-70-2
165 suppliers
$15.00/250mg

314741-40-7
181 suppliers
$9.00/100mg

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 99 percent / sodium carbonate / H₂O; tetrahydrofuran / 20 h / 23 °C
2: 39 g / potassium carbonate / dimethylformamide / 0 - 23 °C
3: 34.3 g / calcium chloride; sodium borohydride / ethanol / 0 - 20 °C
4: 27 g / ethyldiisopropylamine; methanesulfonic anhydride / 1,2-dichloro-ethane / 1 h / Heating
5: 21 g / lithium hydroxide monohydrate / H₂O; ethanol / 1.5 h / Heating

References:

Gao, Hongwu;Renslo, Adam R. [Journal of Organic Chemistry,2007,vol. 72,# 22,p. 8591 - 8592]

314741-39-4 Synthesis

(S)-4-N-Boc-piperazine-2-carboxylic acid methyl ester

314741-39-4
153 suppliers
$8.00/250mg

314741-40-7
181 suppliers
$9.00/100mg

References

848482-93-9 Synthesis

(S)-4-N-BOC-PIPERAZINE-2-CARBOXYLIC ACID

848482-93-9
131 suppliers
$9.00/100mg

314741-40-7
181 suppliers
$9.00/100mg

References

24424-99-5 Synthesis

24424-99-5
864 suppliers
$13.50/25G

126872-94-4
19 suppliers
inquiry

314741-40-7
181 suppliers
$9.00/100mg

References

958635-18-2 Synthesis

(8aS)-Tetrahydro-3-oxo-3H-oxazolo[3,4-a]pyrazine-7(1H)-carboxylic acid 1,1-dimethylethyl ester

958635-18-2
34 suppliers
$64.00/100mg

314741-40-7
181 suppliers
$9.00/100mg

References

(S)-1-Boc-3-hydroxymethyl-piperazine Related Search:

(S)-4-N-Boc-piperazine-2-carboxylic acid methyl ester (R)-N-Boc-piperazine-2-carboxylic acid methyl ester (S)-1-N-Boc-piperazine-2-carboxylic acid methyl ester METHYL 4-BOC-PIPERAZINE-2-CARBOXYLATE (R)-1-BOC-3-(Hydroxymethyl)piperazine (R)-1-N-Boc-2-(hydroxymethyl)piperazine 1-Boc-3-hydroxymethyl-piperazine (S)-1-(((9H-FLUOREN-9-YL)METHOXY)CARBONYL)-4-(TERT-BUTOXYCARBONYL)PIPERAZINE-2-CARBOXYLIC ACID (S)-4-N-BOC-PIPERAZINE-2-CARBOXYLIC ACID

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(S)-1-Boc-3-hydroxymethyl-piperazine synthesis

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