Yield:49621-03-6 2 mg

Reaction Conditions:

with GLUTATHIONE in water at 80; for 24 h;Sealed tube;

Steps:

1

3.5 mg of Alin (manufactured by Funakoshi Co., Ltd.) and 61.5 mg of reduced type glutathione (Wako Pure Chemical Industries, Ltd.) were dissolved in 10 mL of water, placed in a plastic container, sealed, kept at 80 ° C. and reacted for 24 hours It was. After completion of the reaction, this solution was measured using LC / TOF-MS (microTOF 2-kp, manufactured by Bruker-Daltonics), and a mass of 162.0583 was detected as [M + H] + to produce S-allyl cysteine It was confirmed that it was doing. The content of S-allyl cysteine in the aqueous solution was analyzed by HPLC, and it was 0.25 mg / ml. Further, from this aqueous solution, S-allyl cysteine was purified using preparative HPLC to obtain 2.0 mg of a white powder, and its purity was analyzed by HPLC, which was 98%

References:

JP2015/140344,2015,A Location in patent:Paragraph 0032