S(-)-BACLOFEN HCL synthesis
- Product Name:S(-)-BACLOFEN HCL
- CAS Number:63701-56-4
- Molecular formula:C10H13Cl2NO2
- Molecular Weight:250.1217
537676-64-5
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63701-55-3
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63701-56-4
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Yield:-
Reaction Conditions:
Stage #1: ethyl 4-azido-3-(4-chlorophenyl)-2-butenoatewith hydrogen;Ru(II)-(S)-(-)-BINAP in methanol at 50; under 10343 Torr; for 20 h;
Stage #2: with sodium tetrahydroborate;cobalt(II) chloride in methanol; for 0.5 h;
Stage #3: with hydrogenchloride at 100; for 10 h;Title compound not separated from byproducts;
References:
Thakur, Vinay V.;Nikalje, Milind D.;Sudalai [Tetrahedron Asymmetry,2003,vol. 14,# 5,p. 581 - 586]
104-88-1
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63701-56-4
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1615-02-7
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63701-56-4
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63701-56-4
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63701-56-4
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