SINOVA SL-02580 synthesis
- Product Name:SINOVA SL-02580
- CAS Number:357263-13-9
- Molecular formula:C22H22N4O4
- Molecular Weight:406.43
271-63-6
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357263-13-9
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Yield:-
Steps:
Multi-step reaction with 7 steps
1: AlCl3 / CH2Cl2 / 8 h / 20 °C
2: 90.4 percent / K2CO3 / methanol; H2O / 8 h
3: 81 percent / 3-(diethoxyphosphoryloxy)-1,2,3-benzotriazin-4(3H)-one; N,N-diisopropylethylamine / dimethylformamide / 8 h / 20 °C
4: 91 percent / mCPBA / acetone / 8 h
5: HNO3; CF3CO2H / 8 h
6: methanol / 8 h / Heating
7: 5.7 g / PCl3 / ethyl acetate / 8 h / 20 °C
References:
Wang, Tao;Zhang, Zhongxing;Wallace, Owen B.;Deshpande, Milind;Fang, Haiquan;Yang, Zheng;Zadjura, Lisa M.;Tweedie, Donald L.;Huang, Stella;Zhao, Fang;Ranadive, Sunanda;Robinson, Brett S.;Gong, Yi-Fei;Ricarrdi, Keith;Spicer, Timothy P.;Deminie, Carol;Rose, Ronald;Wang, Hwei-Gene Heidi;Blair, Wade S.;Shi, Pei-Yong;Lin, Pin-Fang;Colonno, Richard J.;Meanwell, Nicholas A. [Journal of Medicinal Chemistry,2003,vol. 46,# 20,p. 4236 - 4239]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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357263-13-9
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1000210-73-0
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357263-13-9
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93-58-3
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$13.50/100 mL
357263-13-9
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75336-86-6
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357263-13-9
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