SODIUM 4-HYDROXYBUTYRATE synthesis
- Product Name:SODIUM 4-HYDROXYBUTYRATE
- CAS Number:502-85-2
- Molecular formula:C4H9NaO3
- Molecular Weight:128.1
96-48-0
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502-85-2
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Yield:502-85-2 95%
Reaction Conditions:
with sodium hydroxide at 45 - 60; for 12 h;
Steps:
Compound 1 (25 mL, 0.32 mol) was added to a solution of NaOH (13 g, 0.32 mol) and heated to 45° C. The reaction mass was stirred for 12 hours at 60° C., and then methanol was removed under vacuum. The resulting residue was washed with diethyl ether (2×250 mL) and dried in a dryer at 40° C. for 12 hours, and the yield of product 2 was 38 g (95%).
References:
OBSCHESTVO S OGRANICHENNOI OTVETSTVENNOSTIYU "PHARMENTERPRISES";NEBOLSIN, Vladimir Evgenievich;KROMOVA, Tatyana Alexandrovna US2017/183318, 2017, A1 Location in patent:Paragraph 0215; 0216
28341-54-0
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502-85-2
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$16.00/1mg