tolciclate synthesis
- Product Name:tolciclate
- CAS Number:50838-36-3
- Molecular formula:C20H21NOS
- Molecular Weight:323.45
463-71-8
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50838-54-5
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696-44-6
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50838-36-3
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Yield:50838-36-3 85%
Reaction Conditions:
Stage #1: thiophosgene;6-hydroxy-1,2,3,4-tetrahydro-1,4-methanonaphthalenewith sodium hydroxide in dichloromethane;water at 25; for 1 h;Inert atmosphere;
Stage #2: N-methyl-m-toluidine in dichloromethane at 25; for 0.5 h;Inert atmosphere;
References:
Zhou, Xuan;Ko, Haye Min;Dong, Guangbin [Angewandte Chemie - International Edition,2016,vol. 55,# 44,p. 13867 - 13871][Angew. Chem.,2016,vol. 128,# 44,p. 14071 - 14075,5] Location in patent:supporting information
7507-86-0
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50838-36-3
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139469-06-0
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50838-36-3
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16499-69-7
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