trans-4-Hexylcyclohexanecarboxylic acid synthesis
- Product Name:trans-4-Hexylcyclohexanecarboxylic acid
- CAS Number:38289-30-4
- Molecular formula:C13H24O2
- Molecular Weight:212.33
21643-38-9
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Yield:38289-30-4 85%
Reaction Conditions:
Stage #1: 4-hexylbenzoic acidwith sodium hydroxide;hydrogen in water at 140 - 150; under 22502.3 - 30003 Torr; for 1 h;
Stage #2: with sodium hydroxide in water at 260 - 280; under 22502.3 - 30003 Torr; for 2 h;Further stages.;
References:
Bazurin, Alexey A.;Krasnikov, Sergey V.;Obuchova, Tatiana A.;Danilova, Angelina S.;Balakin, Konstantin V. [Tetrahedron Letters,2004,vol. 45,# 35,p. 6669 - 6672]
