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ChemicalBook CAS DataBase List Tributyltin azide
17846-68-3

Tributyltin azide synthesis

5synthesis methods
A cooled solution of sodium azide (4.10 g, 63.0 mmol) in water (13 mt) at 8°C BusSnCI (17 1 ml) is added dropwise while stirring the solution. After 2h of stirring at 8°C, dichloromethane (38 mi) is added, stirred for another 5 minutes, and phases separated. The water phase is washed with dichloromethane (13 ml). Combined organic phases are washed with 10% NaCI (13 ml) and distilled water (13 ml). The organic phase is dried with sodium sulfate (6.34 g), and the solvent is removed under reduced pressure to give the oily product Tributyltin azide (19.2 g, 91.8%).
Tributyltin azide
-

Yield:-

Steps:

Multi-step reaction with 2 steps

References:

[Gmelin Handbuch der Anorganischen Chemie,Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.1, page 38 - 56]

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