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ChemicalBook CAS DataBase List Tricyclohexyl phosphine
2622-14-2

Tricyclohexyl phosphine synthesis

7synthesis methods
Triphenylphosphine oxide (1 mmol), dry n-hexane (1 mL) and complexed aluminum hydroxide reagent (1 mmol) were added to the Schlenk tube under nitrogen atmosphere and then the reaction was carried out with stirring at room temperature for 10 minutes. The c
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: tetrahydrofuran / 72 h / 20 °C
2: Et3N; tris(trimethylsilyl)silane; 1,1'-azobis(cyclohexane-1-carbonitrile) / benzene / 18 h / Heating

References:

Sato, Akinori;Yorimitsu, Hideki;Oshima, Koichiro [Journal of the American Chemical Society,2006,vol. 128,# 13,p. 4240 - 4241]

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