tridodecyl borate synthesis
- Product Name:tridodecyl borate
- CAS Number:2467-15-4
- Molecular formula:C36H75BO3
- Molecular Weight:566.79
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Yield:-
Reaction Conditions:
in toluene at 130;Dean-Stark;
Steps:
3 Example 3
30,9g boric acid, 279 g dodecyl alcohol and 250mL toluene is added to a 1000ml volume of glass reactor equipped with reflux condenser Dean-Stark trap.
The reaction mixture is heated at 130°C and stirred until stoichiometrical amount of water (27 mL) is collected in the trap (2-3h).
As a result of the reaction, the residual toluene is removed by the suction from the top of the reflux condenser (20-25mmHg).
As a result of this, dodecyl borate remains in the reactor, and the boron ester solidifies upon cooling.
The solid boron ester dissolves in 300mL dichloroethane and a homogenous mixture is acquired.
References:
EP2851362,2015,A1 Location in patent:Paragraph 0036
112-53-8
497 suppliers
$10.00/5g
2467-15-4
6 suppliers
inquiry