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TRIMETHYLSILYL ACETYLENECARBOXYLATE synthesis

2synthesis methods

Yield:19232-22-5 57%

Reaction Conditions:

in 1,2-dichloro-ethane at 65; for 46 h;

References:

Hergott, Hans Herbert;Simchen, Gerhard [Synthesis,1980,# 8,p. 626 - 627]

BIS(TRIMETHYLSILYL)ACETYLENEDICARBOXYLATE PROPARGYLOXYTRIMETHYLSILANE

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