VINYLTRIETHYLGERMANE synthesis
2synthesis methods
- Product Name:VINYLTRIETHYLGERMANE
- CAS Number:6207-41-6
- Molecular formula:C8H18Ge
- Molecular Weight:186.87
Yield:6207-41-6 82%
Reaction Conditions:
in tetrahydrofuran;(Ar); soln. of Mg compd. in THF was added dropwise to soln. of Ge compd.in THF; stirred at 45°C for 24 h; washed (H2O, Et2O); dried (CaCl2); distd.;
References:
Marciniec, Bogdan;LAwicka, Hanna;Dudziec, Beata [Organometallics,2007,vol. 26,# 21,p. 5188 - 5192]
