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ChemicalBook CAS DataBase List Z-LEU-SER-OME
40290-56-0

Z-LEU-SER-OME synthesis

4synthesis methods
-

Yield:40290-56-0 78%

Reaction Conditions:

with benzotriazol-1-ol;1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;N-ethyl-N,N-diisopropylamine in dichloromethane;water at 20; for 18 h;

Steps:

General Procedure: Peptide coupling reaction

General procedure: To a stirred solution of the N-protected amino acid derivative (1.0 eq) in dry CH2Cl2 (50-75 mM)was added EDC (1.3 eq), HOBt·H2O (1.5 eq) and DIPEA (3.0 eq). The solution was stirred at rtovernight, diluted with CH2Cl2 and the organic layer washed twice with 1M HCl(aq), saturatedaqueous NaHCO3(aq) and brine. The organic layer was dried over MgSO4(s) and the solventremoved in vacuo. See individual experiments for details.

References:

Pehere, Ashok D.;Nguyen, Steven;Garlick, Sarah K.;Wilson, Danny W.;Hudson, Irene;Sykes, Matthew J.;Morton, James D.;Abell, Andrew D. [Bioorganic and Medicinal Chemistry,2019,vol. 27,# 2,p. 436 - 441] Location in patent:supporting information

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