ChemicalBook CAS DataBase List Z-PRO-LEU-ALA-NHOH

Z-PRO-LEU-ALA-NHOH synthesis

3synthesis methods

Product Name:Z-PRO-LEU-ALA-NHOH
CAS Number:123984-00-9
Molecular formula:C22H32N4O6
Molecular Weight:448.51

15761-39-4
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: triethylamine (TEA), dicyclohexylcarbodiimide (DCC), N-hydroxybenzotriazole (HOBt) / dimethylformamide; CH₂Cl₂ / 5 °C
2: 81 percent / H₂ / 5percent Pd-C / methanol / 1 h / Ambient temperature
3: HCl / ethyl acetate / 1 h
4: 70 percent / Triethylamine (TEA) / dimethylformamide / a.) -70 deg C to -10 deg C; b.) 4 deg C

References:

Odake;Okayama;Obata;Morikawa;Hattori;Hori;Nagai [Chemical and Pharmaceutical Bulletin,1990,vol. 38,# 4,p. 1007 - 1011]

13139-15-6
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References

L-Alaninamide, N-[(1,1-dimethylethoxy)carbonyl]-L-leucyl-N-(phenylmethoxy)- (9CI)

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123984-00-9
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References

Z-PRO-LEU-ALA-NHOH Related Search:

Z-PRO-GLY-NH2

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Z-PRO-LEU-ALA-NHOH synthesis

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